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當前位置:首頁 > 公司動態 > ICP原子發射光譜儀特點詳解Detailed characteristics of ICP atomic emission spectrometer
ICP原子發射光譜儀特點詳解Detailed characteristics of ICP atomic emission spectrometer
點擊次數:0 發布時間:2016-11-02
 

HK-2000型等離子體單道掃描光譜儀,是多元素順序測量的分析測試儀器。該儀器由掃描分光器、射頻發生器、試樣引入系統、光電轉換、控制系統、數據處理系統、分析操作軟件組成。等離子體是在三重同心石英炬管中產生。炬管內分別以切向通入氬氣,炬管上部繞有紫銅負載線圈〈內通冷卻水〉當高頻發生器產生的高頻電流通過線圈時,其周圍產生交變磁場,使少量氬氣電離產生電子和離子,在磁場作用下加速運動與其它中性原子碰撞,產生更多的電子和離子,在炬管內形成渦流,在電火花作用下形成等離子炬(即等離子體),這種等離子體溫度可達10000k左右。

HK-2000 type plasma single channel scanning spectrometer, is the analysis and testing instrument of multi element sequential measurement. The instrument is composed of a scanning optical splitter, a radio frequency generator, a sample introduction system, a photoelectric conversion, a control system, a data processing system and an analysis operation software. The plasma is in three concentric quartz torch produced. The torch tube respectively in the tangential direction by argon gas, the torch tube upper around copper coil load "in cooling water. When the high frequency generator generates a high-frequency current through the coil, the alternating magnetic field generated around, so that a small amount of argon ionized electrons and ions in the magnetic field accelerated motion and other neutral atom collisions. To produce more electrons and ions, the formation of vortex in the torch tube, forming a plasma torch in EDM (plasma), under the action of the plasma temperature can reach about 10000K.

待測水溶液經噴霧器形成氣溶膠進入石英炬管中心通道。原子在受到外界能量的作用下電離,從較高能級躍遷到基態時,將釋放出巨大能量,這種能量是以一定波長的電磁波的形式輻射出去。不同元素產生不同的特征光譜。這些特征光譜通過透鏡射到分光器中的光柵上,計算通過控制步進電機轉動光柵,傳動機構將分光后的待測元素特征譜線光強準確定位于出口狹縫處,光電倍增管將該譜線光強轉變為電流,再經電路處理和v/f轉換后,由計算機進行數據處理,最后由打印機打出分析結果。

The measured solution by spray forming the aerosol into the quartz torch center channel. When the atom is ionized by the action of the external energy, the energy is released from the higher energy level to the ground state, and the energy is radiated by the form of electromagnetic wave at a certain wavelength. Different elements have different characteristic spectra. The spectral characteristics of shot splitter grating in the lens through the calculation, control the stepper motor rotates through the grating, the transmission mechanism will light after the measured spectral line intensity is accurately located in the exit slit, photomultiplier tube of the spectral line intensity into the current, then processed by the circuit and V / after f conversion, data processing by computer, finally the results printed by the printer.

技術參數:

Technical parameter:

1、分光器系統

1, optical splitter system

光學系統:czerny-turner光學系統焦距:1000mm;

Optical system: Czerny-Turner optical system focal length: 1000mm;

光柵刻線:3600條/mm或2400條/mm離子刻蝕全息光柵;檢測器:光電倍增管;

Grating: 3600 / mm or 2400 / mm ion etching holographic grating; detector: photomultiplier tube;

狹縫:入射狹縫20μm,出射狹縫25μm.

Slit: entrance slit 20 m, exit slit 25 mu m.

光柵刻線:3600條/mm 的分光系統波長掃描范圍是190一500nm;

Grating line: 3600 / mm optical wavelength scanning range is 190 500nm;

光柵刻線2400條/mm的分光系統波長掃描范圍是190一850nm;

Grating 2400 / mm optical wavelength scanning range is 190 850nm;

最小掃描步距0.0005nm;

Minimum scanning step 0.0005nm;

反射鏡:凹型。

Mirror: concave.

2、高頻電源

2, high frequency power supply

電路類型:自激式振蕩電路;頻率:40.68MHz;功率:800一1200W可調;功率穩定度:0.3%;電源:220V 25A。

Circuit type: self excited oscillation circuit; frequency: 40.68MHz; power: 800 a 1200W adjustable; power stability: 0.3%; power: 25A 220V.

3、進樣系統

3, sampling system

炬管部分:石英炬管采用三重同心式,外徑20mm;霧室雙筒型,外徑35mm 霧化器采用同軸型霧化器,外徑6mm;觀察位置:縱向觀察高低和橫向觀察前后,可通過軟件直觀地調整為最佳;氣體控制:99.99%純氬氣通過壓力表輸出;冷卻氣流量計100一1000L/h,輔氣流量計10一100L/h,載氣流量計10一100L/h,載氣壓力表0.4MPa。

The torch tube part: Quartz torch with three concentric, diameter 20mm; double cylinder type spray chamber, the diameter of 35mm atomizer using coaxial type atomizer, the diameter of 6mm; observe the position: longitudinal and transverse observation level of observation, the software can directly adjust for best; gas control: 99.99% pure argon output through a pressure gauge; the cooling air volume of 100 1000L / h, auxiliary gas flow meter of 10 100L / h, the carrier gas flowmeter 10 100L / h, the carrier gas pressure gauge 0.4MPa.

主要特點:

Main features:

采用優良的光學系統,先進的電子控制系統,關鍵部件采用進口元器件,保證了定位準確,信背比高,確保儀器的精確度和靈敏度。

Using excellent optical system, advanced electronic control system, the key components of imported components, to ensure that the positioning accuracy, high precision, to ensure the accuracy and sensitivity of the instrument.

測量范圍:超微量到常量的分析。

Measurement range: ultra micro to constant analysis.

測量精度:RSD≤1.5%。

Measurement accuracy: RSD = 1.5%.

穩定性:RSD≤2.0%。

Stability: RSD = 2%.

分析元素多達72種元素。

Analysis of elements as many as 72 elements.

檢出限低:ppb級。

Low detection limit: ppb level.


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